Torque-Angle Tightening: New Theoretical and Practical Approach

Abstract

Static and dynamic capacities of bolted connections are highly dependent on the preload. For this reason, and due to the inaccuracy of torque tightening technology, many other tightening technologies and preload monitoring have been developed. This paper discusses the concept, the theoretical and the practical approach of the combined tightening method called “Torque-Angle Tightening”. It’s an old tightening technology that consists of a first step to apply a snug torque, then to apply a required angle in a second step. It allows for a more accurate preload compared to the torque tightening. VDI2230 gives some values of the tightening factors for many tightening technologies. This paper provides some new formulas that reduce the error level (difference) between the calculated and real introduced preloads in the bolts. It details some best practices to evaluate the required parameters and to apply the tightening operation correctly. Experimental tests and FE analysis are used to evaluate this improvement of the existing formula.

Share and Cite:

Chaib, Z. and Delcher, C. (2025) Torque-Angle Tightening: New Theoretical and Practical Approach. World Journal of Mechanics, 15, 135-167. doi: 10.4236/wjm.2025.158008.

1. Introduction

Bolting connections are used in all mechanical structures or substructures for different reasons. For critical and structural applications, the bolt’s preload must be correctly introduced to ensure good joint behaviors and to prevent all risks of sliding (micro or macro sliding), contact opening or parting line separation and in other cases to compensate for any preload loosening (thermal loading, creeping, yielding, …) [1]-[3].

Due to the deviations of friction factors, tightening tools and other parameters, the preload is defined by three levels: the nominal level, which is currently used for simplified analysis and the minimum and the maximum levels, which are used for critical analysis. Some references [1] [2] use the tightening factor given by equation (1) to compare the accuracy of all tightening techniques. By using this factor and the table of the VDI 2230 [1], the Torque-Angle tightening is more accurate than the torque tightening. But there is no accurate formula that can be used by designers to define the snug torque and the required angle to achieve the target preload and its accuracy. For steel construction (HR and HV bolts), some simplified tables are provided in the European standard EN 1090-2 [4]. Other simplified formulas are given by Cetim [5], Guillot [6], Alkatan [7], Massol [8] and Bickford [9].

α= Maximal level of introduced load Minimal level of introduced load (1)

Fukuoka [10] gives an advanced calculation of the relation between the applied angle and the preload. According to his papers, the gap between the theoretical calculations and the real introduced preload is mainly due to the settlement that occurs in contact surfaces and geometrical clearance. But according to Gold [11], this gap is due to the elastic assumption used to calculate the resilience (stiffness) of clamped parts and bolts.

To overcome this limitation, two main solutions have been advanced. The first one, used by some industrial companies, consists of performing experimental tests to qualify the optimal snug torque and the total angle to be applied. The second solution consists of performing a tightening up to the yield point (stopping tightening if the torque-angle gradient is down [1]) or over the yield point as developed by Friedrich [12], Chavan [13] and Göran [14]. This solution is commonly used in steel construction and for some automotive applications. Baghua [15] had studied the effect of the snug level on the final preload accuracy. Deepa [16] and Eccles [17] had treated and compared the torque to the combined tightening throw experimental tests.

The yielding tightening offers accurate preload with no equivalent or higher service performance than tightening in the elastic area (70% to 90% YLS) according to fatigue tests made by Kraemer [18].

2. Basic Knowledge about the Combined Tightening

2.1. Measurement of Friction Coefficients in Bolted Connection

The measurement of friction coefficients according to ISO 16047 [19] consists of using a specific test-bench defined by a controlled engine and 6 axis load-cell. After installing a specimen that represents the real assembly, one side of specimen will be locked (the nut, or the bolt head in our case). Then, a regular tightening rotation angle is applied to the second side. The used load-cell measures, the total applied torque “T”, the bearing surface torque of the turned side “Tb”, the thread torque “Tth” (useful torque + friction torque due to the movement between the screw thread and its nut thread), the clamped load “F0”, the applied angle “ θ ” and the tightening time.

Measured torques are defined by equations given below:

  • Bearing surface torque: T b = F 0 × μ b × D b 2 where “Db” is the mean bearing diameter of the turned side. It is done by the medium value of inner and outer diameters of contact surface situated between the turned side and the clamped part.

  • Thread torque: T th = F 0 ( P 2π +0,577× d 2 × μ t ) including the useful torque T u = F 0 × P 2π .

  • Total torque:

T= T b + T th = F 0 ( P 2π +0.577× d 2 × μ t + D b 2 × μ b ) (2)

where, P: thread Pitch.

d2: pitch diameter of the bolt thread: d 2 =d0.6495×P .

d: nominal thread diameter of the bolt.

For each measured point, friction coefficients could be obtained by using equations below:

  • Bearing surface friction coefficient: μ b = T b F 0 × D b 2 .

  • Thread friction coefficient: μ t = T th F 0 P 2π 0.577× d 2 .

Default values used for a non-qualified case is 0.15 ± 0.03 (e.g. Zinc Flake coating).

2.2. Definition of the Snug Torque

During tightening, the measured Torque-Clamp Force graph commonly shows a linear relationship between these factors. But the torque-angle graph shows three main areas:

1) A first non-linear area at the beginning of tightening. In fact, due to geometric defects and roughness, the contact between the parts at this stage is not perfect and not stable. At the moment, no analytical formula or numerical approach can be industrially used to determine this area. The end of this area defines the minimum level of the snug torque.

2) A second linear area shows a linear relationship between Torque-Angle and between Angle-Preload. This area can be represented by an analytical formula detailed in the paragraphs below. Most of the time, designers prefer to work in this area to prevent the assembly exceeding the yield point.

3) A third non-linear area, highly defined by clamped length, bolt design and their material properties (YLS, ULS, A%,…).

As mentioned above, for the snug torque, the designers and operators ignore the first non-linear area. For elastic tightening, this snug torque can be estimated by the torque that introduces a preload close to 30% of the final preload. And for a tightening at or after the yield point, this ratio can achieve 50% ([1], [3] and [12]).

By using the standard ISO 16047 [19], friction values, geometric data of assembly and tightening tool accuracy, the snug torque could be calculated by using Equation (2) as:

T snug = F snug ( P 2π +0.577× d 2 × μ t + D b 2 × μ b ) (2-b)

where: F snug : introduced preload by applying the snug torque.

2.3. Calculation of Required Angle

To calculate the required angle to introduce a target preload, the bolt and clamped parts can be represented by two elastic springs, which can be easily calculated using the listed references [1]-[9] or other equivalent references. Applying any additional preload “ΔF0” will elongate the bolt and will compress clamped parts respectively by “ΔLb” and “ΔLP” given by Equation (3) and Equation (4). And due to the helicoidal shape of the threads, the relative rotation of the nut with respect to the screw “Δθ” will create a relative displacement of the nut “ΔLsn”, calculated by two ways, Equation (5) and Equation (6). Finally, the relationship between the preload and the applied angle is detailed by Equation (7), which illustrates the importance of the thread pitch, the bolt resilience (stiffness), and the clamped parts in addition to the applied angle to calculate the preload. This formula is used in most academic and industrial applications.

Δ L b = F 0 K b = F 0 × δ b (3)

Δ L P = F 0 K P = F 0 × δ P (4)

Δ L sn = P 360 Δθ (5)

Δ L sn =Δ L b +Δ L P (6)

Δ F 0 = P 360×( δ b + δ p ) Δθ (7)

F 0 = T sung P 2π +0.577× d 2 × μ t + D b 2 × μ b + Δθ 360×( δ b + δ p ) P +( P 2π +0.577× d 2 × μ t )× δ b,t (8)

where: F 0 : Bolt Preload.

δ b and δ P : Axial resilience (stiffness) of bolt and clamped parts.

δ b,t : Torsion resilience (stiffness) of bolt.

For very long clamping length, the bolt torsion angle can be significant. For this reason, we (Cetim) have improved the last formula as shown by Equation (8).

3. Experimental and Critical Analysis of Existing Formulas

Because of the negative feedback from French manufacturers to define the appropriate angle and snug torque without experimental qualification, we have performed experimental tests to evaluate the existing formula and gain a better understanding of this tightening technique.

3.1. Experimental Program

This program covers 37 assembly configurations. These configurations were defined with a group of French manufacturers (~60 companies). Figure 1 and Table 1 give a simplified view of the tested assembly configurations. Each tested assembly is defined by a screw or a stud (#1), a nut or a tapped part (#2), 0 to 2 washers (#3) that depend on the tested configuration, a set of clamped parts (#4) and a load sensor (#5) to measure the load in the bolt.

A: Torque-Tension test-bench; B: Tested fasteners; C: specimen used in tensile test; D: Clamped parts and E: illustration of tested configuration where: 1-Screw, 2-Nut, 3-Washer, 4-Clamped parts, 5-Load sensor.

Figure 1. Overview of tested assembly and components.

Table 1. (a): Details of experimental program. (b): Geometric and material data of clamped parts.

(a)

Config ID

Lk/d

Screw or Stud

Washeror Nut

Part 1

Part 2

Part 3

Part 4

Part 5

Part 6

Part 7

CONF_01

2

Screw HR 10.9 - M12x40

Washer HR M12

E1 - S235 J2-1D

CLP 80 KN

E2-S235J2-1D

Washer HR M12

Nut HR M12 10.9

CONF_02

6

Screw HR 10.9 - M12x80

Washer HR M12

E3-S235J2-1D

E4-42CD4 - 2D

CLP 80 KN

E5-42CD4 - 2D

E6-42CD4 - Cale

Washer HR M12

Nut HR M12 10.9

CONF_03

2

Screw HV 10.9 - M12-40/25 PGB

Washer HV M12

E1 - S235 J2-1D

CLP 80 KN

E2-S235J2-1D

Washer HV M12

Nut HV M12 10.9 PGB

CONF_03B

2

Screw HV 10.9 - M12-40/25 PEINER

Washer HV M12

E1 - S235 J2-1D

CLP 80 KN

E2-S235J2-1D

Washer HV M12

Nut HV M12 10.9 PEINER

CONF_04

6

Screw HV 10.9 - M12-80/40 PGB

Washer HV M12

E3-S235J2-1D

E4-42CD4 - 2D

CLP 80 KN

E5-42CD4 - 2D

E6-42CD4 - Cale

Washer HV M12

Nut HV M12 10.9 PGB

CONF_04B

6

Screw HV 10.9 - M12-80/40 PEINER

Washer HV M12

E3-S235J2-1D

E4-42CD4 - 2D

CLP 80 KN

E5-42CD4 - 2D

E7-S235 J2 -1D

Washer HV M12

Nut HV M12 10.9 PEINER

CONF_05

2

Screw HR 10.9 - M24-80

Washer HR M24

E28-M24-S235-2D

Washer HR M24

Nut HR M24 10.9

CONF_06

6

Screw HR 10.9 - M24-130/70

Washer HR M24

E29-M24-S235-5D

Washer HR M24

Nut HR M24 10.9

CONF_07

2

Screw HV 10.9 - M24-80/45

Washer HV M24

E28-M24-S235-2D

Washer HV M24

Nut HV M24 10.9

CONF_08

6

Screw HV 10.9 - M24-130/43

Washer HV M24

E28-M24-S235-2D

E28-M24-S235-2D

E33-M24-S235-cale

Washer HV M24

Nut HV M24 10.9

CONF_09

2

Screw H M12x96-86 10.9 TS FN

Washer 12 300 HV

E1 - S235 J2-1D

CLP 80 KN

E2-S235J2-1D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_10

1

Screw H M12x96-86 10.9 TS FN

Washer 12 300 HV

E17-S600-1D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_11

2

Screw H M12x96-86 10.9 TS FN

Washer 12 300 HV

S600-2D

CLP 80 KN

S600-2D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_12

6

Screw H M12x96-86 10.9 TS FN

Washer 12 300 HV

E17-S600-1D

E4-42CD4 - 2D

CLP 80 KN

E5-42CD4 - 2D

E17-S600-1D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_14

2

Screw H M12x96-86 10.9 TS FN

Washer 12 300 HV

E1 - S235 J2-1D

CLP 80 KN

E2-S235J2-1D

E11-42CD4-2D- (threaded)

CONF_15

2

Screw H M12x96-86 10.9 TS FN

Washer 12 300 HV

E18-2024-2D

CLP 80 KN

E18-2024-2D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_16

6

Screw H M12x96-86 10.9 TS FN

Washer 12 300 HV

E11-2024-2D

CLP 80 KN

E12-2024-2D

E13-2024-2D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_18

2

Screw H M12x96-86 10.9 TS FN

Washer 12 300 HV

E18-2024-2D

CLP 80 KN

E18-2024-2D

E19-2024- (threaded)

CONF_19

2

Screw H M12-40 8.8 TS FN

Washer 12 300 HV

E17-S600-1D

CLP 80 KN

E17-S600-1D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_20

6

Screw H M12-100 8.8 TS FN

Washer 12 300 HV

E17-S600-1D

E4-42CD4 - 2D

CLP 80 KN

E5-42CD4 - 2D

E17-S600-1D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_21

2

Screw Hex-In M12x50 10.9 TS FN

Washer 12 300 HV

E17-S600-1D

CLP 80 KN

E17-S600-1D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_22

2

Screw Hex-In M12x50 10.9 TS FN

E17-S600-1D

CLP 80 KN

E17-S600-1D

Nut M12 ISO 4032

CONF_23

2

Screw Hex-In M12x50 10.9 TS FN

E14-GJS600-2D

CLP 80 KN

E14-GJS600-2D

Nut M12 ISO 4032

CONF_24

2

Screw Hex-In M12x50 10.9 TS FN

E14-GJS600-2D

CLP 80 KN

E14-GJS600-2D

E16-GJS600- (threaded)

CONF_25

6

Screw Hex-In M12x100 10.9 TS FN

E20-GJS600-1D

E21-GJS600-2D

CLP 80 KN

E21-GJS600-2D

E20-GJS600-1D

Nut M12 ISO 4032

CONF_27

6

Screw H M12 élégie 10.9 TS FN

Washer 12 300 HV

E23-S600-1D

E24-42CD4-2D C

CLP 80 KN

E25-42CD4-2D P

E23-S600-1D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_28

6

Screw H M12 PF élégie 10.9 TS FN

Washer 12 300 HV

E23-S600-1D

E24-42CD4-2D C

CLP 80 KN

E25-42CD4-2D P

E23-S600-1D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_29

2

Stud DIN 6379 M12-63 10.9

E22-42CD4- (threaded)

Washer 12 300 HV

E17-S600-1D

CLP 80 KN

E17-S600-1D

Nut M12 ISO 4032

CONF_30A

2

Stud DIN 6379 M12-63 10.9

Nut M12 ISO 4032

Washer 12 300 HV

E17-S600-1D

CLP 80 KN

E17-S600-1D

Washer 12 300 HV

Nut M12 ISO 4032

CONF_30B

6

Stud DIN 6379 M12-125 10.9

Nut M12 ISO 4032

Washer 12 300 HV

E23-S600-1D

E24-42CD4-2D C

CLP 80 KN

E25-42CD4-2D P

E23-S600-1D

Washer 12 300 HV

CONF_31

2

Screw H M12x50 A4-80_Vernis

Flat Washer N 12 304

E26-316-1D

CLP 80 KN

E27-316-1D

Flat Washer N 12 304

Nut H M12 A4-80 + STANAL400

CONF_32

6

Screw H M12x100 A4-80_Vernis

Flat Washer N 12 304

E30-316-2D

CLP 80 KN

E31-316-1D

E30-316-2D

Flat Washer N 12 304

Nut A4 316L 100

CONF_33

2

Screw H M12x50 A4-80_Vernis

Flat Washer N 12 304

E26-316-1D

CLP 80 KN

E27-316-1D

Flat Washer N 12 304

Self-Locking Nut M12 A4-80

CONF_34

2

Screw H M12 A8 (1.4529-80)

Flat Washer 12 300 HV BUMAX A4L

E31-316-1D

CLP 80 KN

E31-316-1D

Flat Washer 12 300 HV BUMAX A4L

Nut A4 316L 100

CONF_35

6

Screw H M12 A8 (1.4529-80)

Flat Washer 12 300 HV BUMAX A4L

E30-316-2D

CLP 80 KN

E31-316-1D

E30-316-2D

Flat Washer 12 300 HV BUMAX A4L

Nut A4 316L 100

CONF_35B

6

Screw H M12 A8 (1.4529-80)

Flat Washer 12 300 HV BUMAX A4L

E30-316-2D

CLP 80 KN

E31-316-1D

E30-316-2D

Flat Washer 12 300 HV BUMAX A4L

Nut H M12 A4-80 + STANAL400

CONF_36

6

Screw bi-hex inco718 75.1

Flat WasherA286

E12-2024-2D

CWF140 kN

E12-2024-2D

Flat WasherA286

Flat WasherA286

Self-Locking Nut Inco 718-Silver Coating

CONF_37

6

Screw bi-hex inco718 75.1

Flat WasherA286

E4-42CD4 - 2D

CWF140 kNn

E4-42CD4 - 2D

Flat WasherA286

Flat WasherA286

Self-Locking Nut Inco 718-Silver Coating

(b)

Ref. Component

Material data

Geometric parameters

Young[MPa]

Coef. Poisson

YLS[MPa]

ULS[MPa]

A[%]

fin[mm]

fout[mm]

Th[mm]

S[mm]

Is Threaded

CLP 80 kN (load sensor)

113 072

0.29

14.1

36

5

CWF140 kN (load sensor)

618 502

0.29

20.9

30.6

13

E1 - S235 J2-1D

204 000

0.29

386

554

29.5

13

50

6.7

44

E11-2024-2D

78 000

0.33

365

466

22

13

110

24

100

E11-42CD4-2D- (threaded)

204 000

0.29

878

1000

18

12

50

30

44

Threaded

E12-2024-2D

78 000

0.33

365

466

22

13

110

19.2

100

E13-2024-2D

78 000

0.33

365

466

22

13

110

24

100

E14-GJS600-2D

160 000

0.26

425

720

10.5

13

50

9.6

44

E16-GJS600-(threaded)

160 000

0.26

425

720

10.5

12

50

24

44

Threaded

E17-S600-1D

245 000

0.29

620

790

21

13

120

9

100

E18-2024-2D

78 000

0.33

365

466

22

13

50

9

44

E19-2024-(threaded)

78 000

0.33

365

466

22

12

50

30

44

Threaded

E2-S235J2-1D

204 000

0.29

386

554

29.5

13

50

6.7

44

E20-GJS600-1D

160 000

0.26

425

720

10.5

13

110

12

100

E21-GJS600-2D

160 000

0.26

425

720

10.5

13

110

19.2

100

E22-42CD4-(threaded)

204 000

0.29

878

1000

18

12

50

24

44

Threaded

E23-S600-1D

245 000

0.29

620

790

21

13

120

9

100

E24-42CD4-2D C

210 000

0.29

643

847

20.5

13

110

19.2

100

E25-42CD4-2D P

210 000

0.29

643

847

20.5

13

110

24

100

E26-316-1D

180 000

0.27

249

565

56.6

13

50

6.7

44

E27-316-1D

180 000

0.27

249

565

56.6

13

50

6.7

44

E28-M24-S235-2D

210 000

0.29

307

509

32.5

26

110

40

100

E29-M24-S235-5D

210 000

0.29

307

509

32.5

26

110

66

100

E30-316-2D

180 000

0.27

249

565

56.5

13

110

19.2

100

E31-316-1D

180 000

0.27

249

565

56.5

13

120

12

100

E33-M24-S235-cale

210 000

0.29

307

509

32.5

26

110

12

100

E3-S235J2-1D

205 000

0.29

307

507

32.5

13

120

12

100

E4-42CD4 - 2D

210 000

0.29

643

847

20.5

13

110

19.2

100

E5-42CD4 - 2D

210 000

0.29

643

847

20.5

13

110

19.2

100

E6-42CD4 - Cale

210 000

0.29

643

847

20.5

13

110

4

100

E7-S235 J2 -1D

205 000

0.29

307

507

32.5

13

120

12

100

E8-S355 J2-1D

204 000

0.26

386

554

29.5

13

50

6.7

44

E9-S355 J2-1D

204 000

0.26

386

554

29.5

13

50

6.7

44

S600-2D

245 000

0.29

620

790

21

13

50

6.7

44

To reduce the number of assumptions regarding material properties and friction values, all materials of tested parts have been qualified with basic tensile tests according to ISO 898-part 1 [20] and part 2 (ISO 6892 [21]) for material properties and according to ISO 16047 [19] for friction coefficients values (bearing surface friction coefficient “μb” and thread friction coefficient “μt”).

Table 1 details the experimental program in which we tested different types of fasteners (studs and screws), different product standards (normal, HR and HV bolts), different providers, different materials, different head shapes, different clamped lengths, …

To reduce the operator-effect during tightening, a specific tool has been designed to tighten the tested assemblies using the Torque-Clamp Force Test-bench (#A of Figure 1). This last one applies a regular angle and measures the applied torque. Additional accessories are used to measure screw elongation (LVDT) and bolt force (load sensor). For each configuration, 5 to 10 assemblies have been tested. All tests are performed by the same operator and by using the same equipment, except for M24 assemblies, which require other tools. Finally, all samples are tightened up to the bolt failure.

3.2. Main Experimental Results

Experimental results are treated in two parts: qualification test-results and tightening test results. For the first part, Figure 2 shows the Stress-Strain graph (mean values) of two material specimens from the same batch. Figure 3 shows the linear relationship between the applied torque and the clamp force. It also shows the deviation of the preload due to friction deviation, for a target preload. All experimental results of those tests are summarized in Table 2 and Table 3.

Figure 2. Example of a tensile tests result—material specimen from Clamped parts.

Figure 3. Example of Torque-Clamp Force test for a Friction qualification.

Table 2. Main tensile test results.

Material reference

Test results

E (MPa)

YLS (MPa)

ULS (MPa)

A%

Stud DIN 6379 M12-125 10.9

210,000

1009

1098

14

Stud DIN 6379 M12-63 10.9

217,000

828

990

12

Screw bi-hex inco718 75.1

205,000

1700

1800

22

Screw Hex-In M12x100 10.9 TS FN

210,000

1078

1129

14

Screw Hex-In M12x50 10.9 TS FN

210,000

1114

1159

13

Screw H M12 A8 (1.4529-80)

150,000

839

1061

16

Screw H M12 PF élégie 10.9 TS FN

200,000

1030

1062

16

Screw H M12 élégie 10.9 TS FN

210,000

1030

1127

15

Screw H M12-100 8.8 TS FN

210,000

820

913

20

Screw H M12-40 8.8 TS FN

210,000

940

1039

15

Screw H M12x100 A4-80_Vernis

180,000

690

913

20

Screw H M12x50 A4-80_Vernis

180,000

660

885

45

Screw H M12x96-86 10.9 TS FN

210,000

1067

1128

15

Screw HR 10.9 - M12x40

207,000

1085

1129

15

Screw HR 10.9 - M12x80

200,000

1083

1124

18

Screw HV 10.9 - M12-40/25 PGB

207,000

1071

1155

16

Screw HV 10.9 - M12-80/40 PGB

210,000

1117

1189

16

2024 T351

78,000

365

466

22

316L

180,000

249

565

56.5

42CD4 - 130 mm

210,000

643

847

20.5

42CD4-2D (threaded)

204,000

878

1000

18

GJS600

160,000

425

720

10.5

S235 J2-130 mm

205,000

307

507

32.5

S235 J2-60 mm

204,000

386

554

29.5

S600

245,000

620

790

21

Table 3. Main tensile test results.

Configuration reference

Test results

Bearing friction (μb)

Thread friction (μth)

Comment

Conf 01-(HR-M12-Lk = 2d)

0.07 ± 0.001

0.08 ± 0.006

Conf 02-(HR-M12-Lk = 6d)

0.08 ± 0.005

0.09 ± 0.008

Conf 03-(HV-M12-Lk = 2d)

0.10 ± 0.033

0.11 ± 0.018

Conf 04-(HV-M12-Lk = 6d)

0.08 ± 0.010

0.13 ± 0.024

Conf 05-(HR-M24-Lk = 2d)

0.07 ± 0.007

0.11 ± 0.009

Conf 06-(HR-M24-Lk = 6d)

0.07 ± 0.001

0.10 ± 0.005

Conf 07-(HV-M24-Lk = 2d)

0.08 ± 0.012

0.12 ± 0.005

Conf 08-(HV-M24-Lk = 6d)

0.07 ± 0.005

0.13 ± 0.013

Conf 09-(H-M12-Lk = 2d)

0.11 ± 0.013

0.14 ± 0.007

Conf 10-(H-M12-Lk = 1d)

0.11 ± 0.013

0.14 ± 0.007

Conf 11-(H-M12-Lk = 2d)

0.11 ± 0.013

0.14 ± 0.007

Conf 12-(H-M12-Lk = 6d)

0.11 ± 0.013

0.14 ± 0.007

Conf 14-(H-M12-Lk = 2d)

0.11 ± 0.013

0.14 ± 0.007

Conf 15-(H-M12-Lk = 2d)

0.11 ± 0.013

0.08 ± 0.007

Conf 16-(H-M12-Lk = 6d)

0.11 ± 0.013

0.14 ± 0.007

Conf 18-(H-M12-Lk = 2d)

0.11 ± 0.013

0.14 ± 0.007

Conf 19-(Hex In-M12-Lk = 2d)

0.15 ± 0.030

0.15 ± 0.030

Assumption

Conf 20-(H-M12-Lk = 6d)

0.15 ± 0.030

0.15 ± 0.030

Assumption

Conf 21-(Hex In-M12-Lk = 2d)

0.12 ± 0.013

0.14 ± 0.006

Conf 22-(Hex In-M12-Lk = 2d)

0.12 ± 0.013

0.14 ± 0.006

Conf 23-(Hex In-M12-Lk = 2d)

0.12 ± 0.013

0.14 ± 0.006

Conf 24-(Hex In-M12-Lk = 2d)

0.12 ± 0.013

0.14 ± 0.006

Conf 25-(Hex In-M12-Lk = 6d)

0.12 ± 0.015

0.14 ± 0.007

Conf 27-(H-M12-Lk = 6d)

0.15 ± 0.010

0.14 ± 0.004

Conf 28-(H-M12-Lk = 6d)

0.10 ± 0.007

0.13 ± 0.005

Conf 29-(Stud-M12-Lk = 2d)

0.14 ± 0.004

0.15 ± 0.011

Conf 30A-(Stud-M12-Lk = 2d)

0.16 ± 0.005

0.15 ± 0.011

Conf 30B-(Stud-M12-Lk = 6d)

0.15 ± 0.006

0.15 ± 0.010

Conf 31-(H-M12-Lk = 2d)

0.13 ± 0.045

0.16 ± 0.020

Conf 32-(H-M12-Lk = 6d)

0.15 ± 0.030

0.15 ± 0.030

Assumption

Conf 33-(H-M12-Lk = 2d)

0.13 ± 0.045

0.16 ± 0.020

Conf 34-(H-M12-Lk = 2d)

0.08 ± 0.017

0.11 ± 0.025

Conf 35-(H-M12-Lk = 6d)

0.15 ± 0.030

0.15 ± 0.030

Assumption

Conf 35B-( H-M12-Lk = 6d)

0.15 ± 0.030

0.15 ± 0.030

Assumption

Conf 36-(BH-M12-Inconel-Lk = 6d)

0.15 ± 0.030

0.15 ± 0.030

Assumption

Conf 37-(BH-M12-Inconel-Lk = 6d)

0.15 ± 0.030

0.15 ± 0.030

Assumption

The second part of results (tightening tests) is presented and discussed in this section and in the validation section of this paper.

Using configuration 1 (clamped length “Lk” ~ 2d where “d” is the nominal diameter), Figure 4 shows the evolution of preload regarding bolt elongation. It shows a large plastique area for HR bolts. This area is mainly defined by the physical and geometrical properties of the tested bolt. We note also some deviations in the elastic area, which could be due to the quality of the contact between the bolt and used sensor LVDT.

Figure 4. Example of a Preload-Bolt elongation: Case of HR M12 bolts.

Graph in Figure 5 gives an example of a bolt elongation (mean values) during the tightening operation. It shows a linear relationship between bolt elongation and applied angle, as well as non-linear behaviors at the start and end of the tightening tests. The first non-linearity is due to the contact between the sensor LVDT and the bolt, and the initial gap at the engaged threads. The second is due to the beginning of the thread stripping (for this case) or bolt yielding.

For the tested configuration shown in Figure 5, by ignoring snugging angle (non-linear behavior), the theoretical rotation of the nut is estimated to

Δθ= Δ L b P ×360= 3.30.6 1.75 ×360=555.4˚ (according to Equation (5)). This rotation is significantly lower than the measured angle (662.3˚ − 40.6˚ = 621.7˚). This

difference is mainly due to the tool resilience (stiffness) and its accessories (sockets, extension…). It demonstrates that the real assembly is more flexible than the calculated one (theorical assembly). And it confirms the existence of an additional resilience (Table 2). This conclusion is mentioned by Fukuoka [10] and Gold [11]. The first author improved the resilience formula by adding a non-linear contact resilience. The second gives other explanations based on the local stress and the elasto-plastic properties of the material, which will be investigated later. In fact, and according to two different papers of Fukuoka ([10] and [20]), we can see a good correlation between theorical approach and experimental results. But in the first paper, he considers the roughness effect on the additional contact resilience, and he ignores this factor in his second work (based on a specific axisymmetric FEA model).

Figure 5. Bolt elongation during the tightening of conf. #12 (bolted joint M12, Lk = 6d).

Graphs of Figure 6 and Figure 7 illustrate the importance of the resilience (stiffness) of the bolt and clamped parts, defined mainly by the length and the Young modulus. It shows that the higher the clamped length ratio (Lk/d), the more the bolt has to be turned to install required preload. This reduces the sensitivity of the angle factor on the applied preload. In fact, for a stiff assembly (LK close to 2d), any error of ±10 degrees on applied angle introduces a preload deviation of ±10 kN against ~±5 kN in the case of a highly elastic assembly (Lk = 6d).

Figure 6. Evolution of applied load during nut rotation—case of 2 different clamped lengths.

Figure 7. Evolution of applied load during nut rotation - case of different part-materials.

Figure 8. Tightening and untightening steps of a bolted joint M12 (Config. #1).

The graphs in Figure 8 show the evolution of applied torque and introduced load as a function of applied angle. From those graphs we can note:

  • The tightening step is defined by two types of behaviors: a non-linear behavior “Torque-Angle” and “Preload-Angle”, and linear behavior before any yielding phenomenon. These graphs demonstrate the importance of the snug torque in the beginning of the tightening where the relationship between the applied torque and introduced angle is non-linear.

  • The untightening step has a different slope “Preload-Angle” compared to the tightening step. This demonstrates that the typical formula used to qualify the relationship between angle and preload ( Δ F 0 = P×Δθ 360×( δ b + δ p ) ) is wrong. This is due to there being no evolution of resiliencies or thread Pitch between the tightening and untightening steps.

The graphs of Figure 9 show a limited effect of the thread pitch on the applied angle. In fact, the use of a fine pitch increases the required angle to introduce a similar load compared to a coarse pitch. This effect may be more significant in the case of a stiff assembly. Indeed, for a clamped length Lk = 6d, to introduce 39.6 kN, using a fine pitch (1.5 mm) increases the required angle by only 4˚ (36˚ instead of 32˚).

Figure 9. Effect of the pitch on a combined tightening (bolted joint M12, Lk = 6d).

The graphs in Figure 10 show the same behavior of two similar assemblies where only the nut has been modified. It demonstrates that for a snug torque higher than the locking torque, the combined tightening can ignore the locking torque effect. But for higher locking torque, this observation may be wrong.

Finally, using test-results of the Torque-Clamp Force qualification according to ISO 16047 (Bolt HR 10.9 M12x40), we can note a significant evolution of the basic relationship between bolt preload and Torques (bearing surface torque, thread torque and total torque) after the yielding of the bolt as shown in Figure 11. According to these graphs, the linear relationship between torques and bolt preload is only valid before the yield point of the bolt. This means the friction coefficient at the bearing surface (Figure 11(c)) and on the threads (Figure 11(d)) decreases after bolt yielding. In this paper, this evolution will be ignored by the proposed model (below) when extended to plastic tightening. And it will be developed in future work.

Figure 10. Effect of the locking torque on combined tightening (bolted joint M12, Lk = 2d).

(a) Preload = f(Angle) (b) Preload-Total torque = f(Angle)

(c) Preload-bearing torque = f(Angle) (d) Preload-Thread torque = f(Angle)

Figure 11. Comparatives evolutions of bolt preload and torques as a function of turned angle.

4. Improvement of Existing Formulas

In this section, we detail some of the improvements made to existing formulas, taking into account the previous analysis.

4.1. Improvement of the Preload-Angle Formula

Figure 12 illustrates the difference between the measured angle and the effective angle, which generates a relative rotation between the nut and the bolt. We can note that the measured angle is the sum of 3 different rotations.

Δθ=Δ θ tool +Δ θ b,Torsion +Δ θ u (9)

1) Δ θ tool : Torsion rotation (angle) of the tool and its accessories. Some automatic screw drivers compensate for this quantity. At the end of this paper, we propose a simplified way to qualify the tool stiffness/resilience.

Δ θ tool = ΔT K tool =Δ F 0 ×( P 2π +0.577× d 2 × μ t + D b 2 × μ b )× δ tool (10)

2) Δ θ b,Torsion : Torsion rotation (angle) of the bolt. The torsion resilience/stiffness of the bolt can be calculated in the same way as axial and bending resilience.

Δ θ b,Torsion = T thread K b,Torsion =Δ F 0 ×( P 2π +0.577× d 2 × μ t )× δ b,t (11)

3) Δ θ u , useful angle

Δ θ u = Δ F 0 K θ =Δ F 0 × 360×( δ b + δ p ) P (12)

With Equations (8) to (12), we can deduce the final formula (13).

F 0 = T sung P 2π +0.577 d 2 μ t + r b μ b + Δθ 360( δ b + δ p ) P +( P 2π +0.577 d 2 μ t ) δ b,t +( P 2π +0.577 d 2 μ t + D b 2 μ b ) δ tool (13)

Figure 12. Applied and measured tightening-Angle.

This final formula shows all the factors influencing the relation between the bolt preload, snug torque and the applied angle ( Δθ ). It adds the effect of friction, and additional factors that may be ignored in some cases.

4.2. Improvement of Clamped Part-Resilience Formula

Based on the results of Gold [11] and of Fukuoka [22], we have performed an axisymmetric FEA model (Figure 13). We were interested in the evolution of part compression under a tightening load of 59.6 kN. The graph of Figure 14 shows the evolution of the axial displacement of the parts at the hole from the head (axial position Z = 22) to the nut (axial position Z = 62). It shows that a significant portion (more than 50%) of part compression is obtained with two local areas located at the interface in contact with the fastener up to a depth of 6 mm.

According to VDI 2230 approach, the part compression is detailed in Table 4.

Table 4. Calculation of the axial resilience of clamped parts.

Input data

DP (mm)

Lk (mm)

Dw (mm)

Dh (mm)

Ep (MPa)

60

40

16.63

13.5

210,000

Calculated data

D P * = D P D w

L k * = L k D w

tanφ=0.362+0.032ln( L k * 2 ) +0.153ln D p *

Cone angle (°)

3.61

2.41

0.5642

29.43°

Total part resilience (mm/N)

δ P =2× ln[ ( d w + D h )×( D w + L k ×tanφ D h ) ( D w D h )×( D w + L k ×tanφ+ D h ) ] E p ×π× D h ×tanφ =6.154e7

Using the preload and the FEA displacement at the hole edge, the local resilience is calculated at 1.29e−6 mm/N. Using the preload and the difference between the mean displacement under the bearing surfaces (bolt head and under the nut), the mean FEA resilience is equal to 9.36e−7 mm/N, that is closer to the analytical calculated resilience.

Figure 13. FEA analysis-description of analyzed assembly.

Due to the difference between analytical and FEA results, we can assume that the part resilience to be used during tightening is different to that used for load factor calculations. According to Alkatan [7] and Massol [8], the part resilience calculation is based on elastic energy of the part. This resilience gives only a mean part-compression. With regard to the surface contact between bolt head and part, we can assume that this contact is a Herz contact. As a consequence, the full parts resilience during tightening can be calculated by Equation (14).

Figure 14. FEA analysis-evolution of part compression at the bolt hole.

Figure 15. FEA analysis-evolution of part compression along the bolt hole: cases of 3 Dp.

Figure 14 and Figure 15 demonstrate that the compression of the clamped parts is defined by a mixture of Hertzian and normal elongations.

δ P = δ P,Elastique( NFE,VDI, ) + δ P,Hertz (14)

δ P,Hertz = 1 ν 2 D w,eq × E eq (15)

Where equivalent Young modulus

E eq = 1 1 E P,i + 1 E P,i+1 (16)

And Equivalent diameter:

D w,eq = d w 2 d h 2 (17)

Finally, the simplified method consists of calculating the parts resilience according to the basic approach (VDI 2230 [1], Alkatan [7], Massol [8], Bickford [23] or Rasmussen [24]...) and adding Hertz resilience for the smallest contact surfaces.

4.3. Calculation of Maximal Snug Torque to Achieve Target Accuracy

Today, maximum snug torque is defined by experience or by practical rules. These rules specify 25% to 30% of maximal target preload should be introduced by the snug torque.

In this section, we determine the maximal snug torque to achieve any final tightening factor (“α” as defined by VDI 2230 [1] and Equation (18)). At first, we suppose the maximal preload “ F 0 + ” and tightening factor “α” are known (e.g. F 0 + =80%YLS and α = 1.4), then we calculate the required snug torque.

The deviation of the final preload (introduced by angle and by the snug torque) and of snug preload can be calculated respectively by Equation (19) and Equation (21). The combination of Equation (18) and Equation (21) defines the maximum preload to be introduced by the snug torque (Equation (22)). Finally, the snug torque (Equation (23)) can be calculated using any formula describing the relationship between torque and preload (ISO 16047 or equivalent).

α= F 0 + F 0 (18)

Δ F 0 = F 0 + F 0 =( 1 1 α )× F 0 + (19)

α sung = F 0,snug + F 0,snug (20)

Δ F 0,snug = F 0,sung + F 0,sung Δ F 0 (21)

F 0,snug + ( 1 1 α ) ( 1 1 α sung ) × F 0 + (22)

T sung = F 0,sung + 1+ ΔT T ×( P 2π +0.577× d 2 × μ th + D b 2 × μ b ) (23)

Equation (22) demonstrates the importance of the snug torque accuracy, on the final preload accuracy. For industrial applications, the snug-tightening factor can be estimated at 2 ( 1.5< α sung <2.5 ) and the final tightening factor for combined tightening is estimated between 1.2 and 1.4. In this case, the snug torque/preload should not exceed 33% to 57% of the final Torque or Preload.

Figure 16. Evolution of the snug ratio (F0,snug/F0) as a function of the snug and target tightening factors (αSnug and α).

According to the graph in Figure 16 (Equation (22)), an accurate tightening using combined tightening (α < 1.1), requires a very low snug ratio. However, using a low snug ratio could cause the tightening preload to fall within the non-linear range of the angle-preload relationship, which is another source of final preload-deviation. In other case, for a higher level of the tightening factor, the snug-Preload could be closed to the target preload (e.g. α sung =α=1.6 ). In this case, combined tightening offers no advantage.

4.4. Experimental Qualification of the Stiffness of the Tightening Tool

To measure the stiffness of the tightening tool and its accessories (socket, extension, adapters…), several experimental ways can be used. Below, we propose a simplified method which can be used. It consists of recording the torque and the angle during the bolt tightening at any torque-level (close to the bolt’s maximum capacity) and during the untightening step, as shown in Figure 17.

The torsion stiffness of the tool used to tighten the bolt is determined by the “torque-angle” slope during the untightening (or re-tightening) operation before any relative rotation between the nut and the screw. In our case, the stiffness of the tightening tool, as shown in Figure 17 (during the untightening step), is equal to 24 Nm/˚.

This stiffness should be ignored when using a servo-controlled screwdriver, which anticipates this additional rotation due to its accessories.

Figure 17. Measurement of the tightening tool stiffness and its accessories.

4.5. Extension of Work for a Tightening after the Yield Point

The tightening after the yield point consists of tightening bolts beyond their elastic capacities. This leads to strain hardening of the screw material (on its critical/threaded area). Friedrich [12] presented a simplified approach to define the angle and the snug torque for this kind of tightening. The tightening after the yield point allows for a significant deviation in the applied angle and reduces the effect of any inaccuracy in the snug torque.

In our study, we adjusted the existing approach using the real S-S curve of the bolt.

This extension is described by the calculation steps detailed below:

1) We transform the body of the fastener into a set of cylinders or shanks (threaded and unthreaded shanks).

2) For any target preload “F0”, we calculate the relative nut-bolt rotation as described below:

a) We calculate the equivalent (Von Mises) stress (combination of axial and torsional stress) in any critical shank.

b) Using Neuber correction and bolt stress-strain curve, we calculate the real stress and strain in the critical shank.

c) From the calculated “real stress”, we calculate the residual preload.

d) From the calculated strain, we calculate the shank elongation.

e) We perform the same calculation for all other shanks using the residual preload.

f) The total bolt elongation can be calculated by summing all shank-elongations.

g) Using the parts resilience and the residual preload, we calculate the clamped-parts elongation.

h) Finaly, the nut rotation “ θ F 0 ” can be calculated using the bolt and parts elongations, torsion angle of the bolt-body and the additional angle introduced by tightening-tool-accessories.

2) With the snug torque “ T snug ”, we calculate the snug preload by using the ISO 16047 formula (formula 2 [19]).

3) We perform the same calculation for the snug preload “ T snug ” (step 2) to calculate the snug angle “ θ snug ”.

4) Finally, the final combined tightening will be defined by “ T snug +Δθ ”, where the final angle to be applied is defined by Equation (24).

Δθ= θ F 0 θ sung (24)

This extension will be developed in another paper discussing the fatigue behavior of yielded assemblies, where S. Gold [11] demonstrated the performance of these assemblies in this case.

5. Experimental Validations of the New Formulas

To validate this work, we have developed a numerical tool and a database containing all experimental data, sample parameters (geometric and material data) and all configuration definitions. This tool calculates all required factors and plots theoretical “preload-angle” curves according to our detailed development. Then it adds the experimental curves to the same graph. It optimizes the number of points to plot the experimental results by reducing the linear area to two points that define the beginning and the end of this area with an accuracy of less than 2%.

Due to the high number of tightening tests performed for each configuration, and to improve the graphs quality, only statistical curves (average and average ±2 Std.Deviation) will be presented to summarize the experimental results for each tested configuration. For the theoretical curves, only maximal and minimal preload-angle curves will be plotted to evaluate the performance of this model. The maximum and minimum levels of preload (F0_Max and F0_Min) are calculated respectively by these combinations (maximum level of snug torque and minimum level of frictions) and (minimum level of snug torque and maximum level of frictions).

To amplify the error between the experimental results and the calculated results, we consider a zero deviation of the preload from the snug torque for the experimental results (for all tests), the zero angle will be set when preload is equal to 20 kN for M12 et 50 kN for M24.

Finally, to plot the graphs below, we used:

  • A snug preload for all tested configurations: ~25% YLS x As.

  • Torque tightening accuracy (to apply the snug torque): ±10%.

  • Additional tightening tool stiffness: 24 Nm/˚ (see §4.4).

  • Default friction coefficient used for the configuration where the Torque-Clamp Force relationship was not qualified: 0.15 ± 0.03.

  • Minimal YLS and ULS values according to ISO 898-1 [20] for bolt and studs which no Tensile test was performed.

  • A theoretical bi-linear material for most bolts that hadn’t been qualified according to IS0 898-1.

The theoretical curves are obtained by gradually increasing the target preload. Appendix 1 presents all the comparative graphs between the calculated preload (F0_Max and F0_Min) and the experimentally measured preload (Exp. Avg, Exp. Avg. + 2stdDiv and Exp. Avg. - 2stdDiv, where Avg. means the average value of all tested specimens and stdDiv is the standard deviation) as shown in Figure 18.

Figure 18. Example of validation graph (Conf 01: HR-M12-Lk = 2d).

For almost all tested configurations, the theoretical and experimental graphs overlap. This illustrates the reliability of the proposed approach.

The theoretical and experimental results confirm basic recommendations used for combined tightening, as reminded below:

1) Use of an “elastic” assembly by increasing the ratio Lk/d (clamped length / nominal diameter). This rule is confirmed by many tested configurations (e.g. Conf 01 & 02; 03 & 04; 10, 11 & 12,…) which illustrate that the required angle for any specified Preload is greater for a higher ratio. This means that any deviation from the applied angle results in a limited deviation from the preload.

2) Using a snug torque to introduce ~20% to 30% of the final preload. This rule is demonstrated by all tests, which show a non-linear relationship between the applied angles and the preload.

3) Accurate combined tightening is achieved by tightening after the yield point. This rule is illustrated by the horizontal slope for assemblies with a ratio Lk/d = 6. In reality, after the yield point and before damaging the bolt (ULS), all applied angle is transformed into metal strain hardening without any significant evolution of the preload.

Finally, the graphs presented in the appendix demonstrate the performances of the proposed model for any elastic combined tightening. To use this model for yielding tightening after the yield point, the user must:

a) Use accurate stress-strain curves for their bolts.

b) Use accurate (measured) friction values on the bearing surface and on the threads.

c) Use stiff tools and accessories. Else, it is necessary to measure the tool stiffness.

Figure 19 gives a comparative graph between existing (“Old”) and improved formula (“New”). It shows the effect of the Hertzian resilience and the additional resilience coming from tool accessories. By limiting analysis to linear area and using the worst configuration for a combined tightening (Lk = 2d), Figure 19 shows that the “Old” approach overestimates clamped load at 36%, that was mentioned approximately by GOLD [11]. In addition, it shows that, the improvement of the calculation of part resilience reduces significantly the gap between analytical and experimental results (10%). In other words, by adding Hertzian effect, the part resilience is highly increased (3.73 × 107 - 1.45 × 106 mm/N).

Figure 19. Comparative analysis between old and proposed formulas (Conf 01: HR-M12-Lk = 2d).

6. Conclusions

This paper discusses combined Torque-Angle tightening. It provides a new analytical approach that takes into account local and Hertzian contacts under the fastener bearing surfaces (bolt head or nut) or other small surfaces, additional rotation (torsion angle) due to the tool and its accessories, which could be ignored when using very stiff tools, as well as the elastoplastic behavior of the bolt. These improvement factors are demonstrated by numerical and experimental analysis.

An extensive experimental study was performed with more than 37 tests, each involving 5 to 10 tightening operations (without any reuse of bolts). In addition to the tightening tests, other qualification tests were performed: material properties (tensile tests according to ISO 898-1 and ISO 6892-1) and qualification of friction coefficients (thread friction coefficient and bearing surface friction coefficient with Torque-Clamp force test according to ISO 16047).

Despite the simplified qualification of tool stiffness, the validation curves demonstrate the performance of the new proposed formula to improve the preload accuracy on bolted assemblies when using combined Torque-Angle tightening.

Finally, this paper proposes another way to calculate maximum snug torque in order to achieve the target preload accuracy (or target tightening factor).

Appendix

This appendix provides all comparative graphs “Clamp Force (N)/Angle (˚)” used to validate proposed model for all tested configurations.

Conf 01-(HR-M12-Lk = 2d: μb = 0.07 ± 0.001; μt = 0.08 ± 0.006)

Conf 02-(HR-M12-Lk = 6d: μb = 0.08 ± 0.005; μt = 0.09 ± 0.008)

Conf 03-(HV-M12-Lk = 2d: μb = 0.10 ± 0.033; μt = 0.11 ± 0.018)

Conf 04-(HV-M12-Lk = 6d: μb = 0.08 ± 0.010; μt = 0.13 ± 0.024)

Conf 05-(HR-M24-Lk = 2d: μb = 0.07 ± 0.007; μt = 0.11 ± 0.009)

Conf 06-(HR-M24-Lk = 6d: μb = 0.07 ± 0.001; μt = 0.10 ± 0.005)

Conf 07-(HV-M24-Lk = 2d: μb = 0.08 ± 0.012; μt = 0.12 ± 0.005)

Conf 08-(HV-M24-Lk = 6d: μb = 0.07 ± 0.005; μt = 0.13 ± 0.013)

Conf 09-(H-M12-Lk = 2d: μb = 0.11 ± 0.013; μt = 0.14 ± 0.007)

Conf 10-(H-M12-Lk = 1d: μb = 0.11 ± 0.013; μt = 0.14 ± 0.007)

Conf 11-(H-M12-Lk = 2d: μb = 0.11 ± 0.013; μt = 0.14 ± 0.007)

Conf 12-(H-M12-Lk = 6d: μb = 0.11 ± 0.013; μt = 0.14 ± 0.007)

Conf 14-(H-M12-Lk = 2d: μb = 0.11 ± 0.013; μt = 0.14 ± 0.007)

Conf 15-(H-M12-Lk = 2d: μb = 0.11 ± 0.013; μt = 0.08 ± 0.007)

Conf 16-(H-M12-Lk = 6d: μb = 0.11 ± 0.013; μt = 0.14 ± 0.007)

Conf 18-(H-M12-Lk = 2d: μb = 0.11 ± 0.013; μt = 0.14 ± 0.007)

Conf 19-(Hex In-M12-Lk = 2d: μb = 0.15 ± 0.030; μt = 0.15 ± 0.03)

Conf 19-(Hex In-M12-Lk = 2d: μb = 0.11 ± 0.013; μt = 0.08 ± 0.006)

Conf 20-(Hex In-M12-Lk = 6d: μb = 0.15 ± 0.030; μt = 0.15 ± 0.03)

Conf 20-(H-M12-Lk = 6d: μb = 0.11 ± 0.013; μt = 0.08 ± 0.006)

Conf 21-(Hex In-M12-Lk = 2d: μb = 0.12 ± 0.013; μt = 0.14 ± 0.006)

Conf 22-(Hex In-M12-Lk = 2d: μb = 0.12 ± 0.013; μt = 0.14 ± 0.006)

Conf 23-(Hex In-M12-Lk = 2d: μb = 0.12 ± 0.013; μt = 0.14 ± 0.006)

Conf 24-(Hex In-M12-Lk = 2d: μb = 0.12 ± 0.013; μt = 0.14 ± 0.006)

Conf 25-(Hex In-M12-Lk = 6d: μb = 0.12 ± 0.015; μt = 0.14 ± 0.007)

Conf 27-(H-M12-Lk = 6d: μb = 0.15 ± 0.010; μt = 0.14 ± 0.004)

Conf 28-(H-M12-Lk = 6d: μb = 0.10 ± 0.007; μt = 0.13 ± 0.005)

Conf 29-(Stud-M12-Lk = 2d: μb = 0.14 ± 0.004; μt = 0.15 ± 0.011)

Conf 30A-(Stud-M12-Lk = 2d: μb = 0.16 ± 0.005; μt = 0.15 ± 0.011)

Conf 30B-(Stud-M12-Lk = 6d: μb = 0.15 ± 0.006; μt = 0.15 ± 0.010)

Conf 31-(H-M12-Lk = 2d: μb = 0.13 ± 0.045; μt = 0.16 ± 0.020)

Conf 32-(H-M12-Lk = 6d: μb = 0.15 ± 0.030; μt = 0.15 ± 0.030)

Conf 33-(H-M12-Lk = 2d: μb = 0.13 ± 0.045; μt = 0.16 ± 0.020)

Conf 34-(H-M12-Lk = 2d: μb = 0.08 ± 0.017; μt = 0.11 ± 0.025)

Conf 35-(H-M12-Lk = 6d: 0.15 ± 0.030; μt = 0.15 ± 0.030)

Conf 35B-(H-M12-Lk = 6d: 0.15 ± 0.030; μt = 0.15 ± 0.030)

Conf 36-(BH-M12-Inconel-Lk = 6d: 0.15 ± 0.030; μt = 0.15 ± 0.030)

Conf 37-(BH-M12-Inconel-Lk = 6d: 0.15 ± 0.030; μt = 0.15 ± 0.030)

Conflicts of Interest

The authors declare no conflicts of interest regarding the publication of this paper.

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