The study area is located between Latitudes 5˚40' and 6˚50' N and Longitudes 6˚50' and 7˚50'E (Figure 1), which encloses a major part of Ihube community in SE Nigeria. The Ikpankwu section is a quarry site for sand aggregates while the

KM 75 Section was created by the road traversing the Port Harcourt-Enugu express way. The area was chosen for this study because it is very accessible and the road trending NE-SW, i.e. strike of the deposits in the area ensured the exposure of many lithostratigraphic units deposited in the southern Anambra Basin.

The tectonic and geologic history of Nigerian sedimentary basins including the Anambra Basin followed the break-up of the South American and African continents in the Early Cretaceous [12] [13]. The stratigraphic history of the region has been well documented [12] [14] [15]. The Late Cretaceous stratigraphic succession in the basin began with Campanian-Maastrichtian Nkporo Shale and its lateral equivalent: the Enugu Shale and Owelli Sandstone. These basal units are overlain successively by the Early-Middle Maastrichtian Mamu Formation (Lower Coal Measures), the Middle Maastrichtian Ajali Sandstone and the Nsukka Formation (Upper Coal Measures) which extends from the Late Maastrichtian into the Danian. The Tertiary succession consists of the Palaeocene Imo Shale. These lithostratigraphic units are spatially distributed in the study area (Figure 2).

The strategy adopted in the study involved the extraction of characteristic lithological and other physical motifs extracted from the 2 stratigraphic sections. The

lithofacies and local facies summaries were interpreted by considering possible depositional processes that might have given rise to the features as indicated by the observed inherent primary sedimentary structures, textures and stacking patterns in the units. The Embedded Markov Matrix was thereafter utilized to establish facies relationships [17] [18].

The Embedded Markov Matrices utilized in the study involved 1) Erection of transition count matrix for each section 2) Tabulation of transition probability matrix 3) Tabulation of independent trial probability matrix and 4) Erection of difference matrix,

The three matrices (observed transition probability, random probability and difference probability) were calculated from transition count matrix using the following formulae:

P i j = F i j / R t , (1)

where P_ij is observed transition probability of i being followed by j; F_ij is the number of transitions of i to j; R_t is the row total [15].

R i j = n j / N – n i , (2)

where r_ij is the random probability of transition from facies i to facies j, n_i and n_j are the number of occurrences of facies i and j respectively; and N is the total number of occurrences of all facies [18].

D i j = P i j – r i j , (3)

where d_ij is the difference between the observed probability (P_ij) and the random probability (r_ij) [18] [19].

At the end of the analysis, a composite facies relationships diagram (local summary) was established using the result of the difference matrix, which gave a better understanding of the structure of the raw data and facies relationship diagrams that were used as basis for overall interpretation of facies in terms of depositional environment. Interpretations using established facies affinities/associations and the comparison of obtained local summaries with established facies models also helped in the interpretation of EODs of the studied units.

Five samples were selected for micro faunal analysis. The preparation and analysis of each of the samples were carried out using the procedures outlined in [20]. The absolute ages of the units were also obtained via correlation to [20].

100 g of each sample was broken into chips and placed in an aluminum bowl containing two (2) teaspoonful of anhydrous sodium carbonate and sufficient quantity of 10% concentrated hydrogen peroxide. The mixture was then heated on a hot plate until the sample was completely smeared on boiling and then put off and allowed to cool. The sample was washed under a gently running tap through a set of three (30-, 60- and 200-μ) sieve meshes. Residues from each fraction were dried in an oven at about 80˚C. The dried samples were individually studied under Zeiss binocular stereomicroscope for micro faunas such as foraminifera and ostracods.

The selected five shale samples for floral analysis, were analysed using the procedures expounded in [21]. Hydrochloric acid, 36% in concentration was added to the selected sample until effervescence stopped. This ensured the removal of all carbonates. Then 40 ml of HCL was added and heated to remove the silica fluoride gel; Methanol was then added to separate the sample debris. Five to seven drops of Nitric acid was added to oxidize the residue, which cleaned the palynomorphs and removed the lignin. Potassium hydroxide was thereafter added to neutralize any acid present. Two to three drops of Safranin O was added before sieving, then centrifuging was done to the solution. A small quantity of the residue was then pipetted out, dried and placed on the slide for microscopic identification.

The result of units that were later grouped into lithofacies types delineated in this study are briefly summarised in the subsections below, while the lithologs and detailed descriptions of each of the units are shown in Figure 3 and Figure 4. Representative outcrop sections and some identified facies are shown in Figure 5.

Planar cross bedded sandstone facies A

Facies A was identified in the two locations studied. It is comprised of medium to coarse grained, poorly to moderately sorted sandstone with low to medium angle cross beds, whose fore sets are draped with mud (Figure 5(d)). It has sharp contacts with the overlying mudstone facies. The thickness of the facies is about 2 m. The planar cross bedded sandstone facies is (A) is ferruginized at the top in both locations.

Massive sandstone facies B

This facies is white to pink in color, moderately to poorly sorted, fine to medium grained Sandstone. The absence of any observable sedimentary structure may be the result of continuous high energy of deposition or its structure may have been destroyed by massive bioturbation.

Mudstone facies C

This facies was delineated only at the Ikpankwu quarry location. It is light grey in color, slightly bioturbated with an average thickness of about 2 m.

Bioturbated Sandstone facies D

This facies is ubiquitous in both locations. It showed imprints of trace fossils especially, burrows belonging to Skolithos ichnogenera. The lithofacies is often

ripple bedded and ferruginized. Texture is fine to medium grained with an average thickness of 2.5 m.

Trough cross bedded sandstone facies E

This facies was observed only at the Km 75 section and displayed fore sets that are curved and abruptly terminate tangentially with the lower bedding surface. The texture of the facies is fine to medium grained sandstone. This facies has been associated with dune migration.

Dark grey laminated shale facies F

This facies was also observed at the km 75 section. It is comprised of dark grey and fissile shale with lots of pyritic concretions. Weathered exposures easily give off yellowish colouration due to the iron content (Figure 5(a)).

Shale/Siltstone facies G

This facies was observed at the Ikpankwu quarry site. It is comprised of shale/siltstone interbeds with flaser bedded characteristics. It is often bioturbated.

Shale/Mudstone facies H

This facies showed interbeds of shale and mudstone units with the thickness of the mudstone unit increasing up section indicating a shoaling up. The lower shale units are pyritic (Figure 5(c)).

Horizontally bedded Sandstone facies I

This facies consists of beds of fine grained sandstone that alternate with siltstone (Figure 5(b)). The facies is fine to medium grained often ripple bedded with an average thickness of 2 m.

Figure 6 and Figure 7 show the facies relationship diagrams (FRDs) of the two lithosections in KM 75 and Ikpankwu, respectively. The FRDs were erected based on observed facies transitions in the two sections (Figure 3 and Figure 4). Tables 1-8 on the other hand show the computed transition count matrix, observed transition probabilities, transition probabilities and difference matrix for the two lithosections of the study area.

The composite facies relationship diagrams (Figure 8 and Figure 9) for the respective sections constructed using the difference matrix (Table 4 and Table 8) gave a better understanding of the structure of the raw data and finally, a facies relationship diagram that can be used as a basis for overall interpretation of facies in terms of depositional environment, was realised.

The result of foraminiferal analysis revealed that the study area is rich in benthonic forams, but devoid of planktonic Forams (Figure 10). Age interpretation

Rt = Row Total, Ct = Column Total, A-I = Facies.

was therefore based on the arenaceous assemblages identified in the analyzed samples. The identified forms include: Ammobaculites coprolithiformis, Haplophragmoides sahariense, Ammobaculites amabensis, Haplophragmoides talokaense, Trochamina dutsuna and Anomalinoides midwayaensis and Ammobaculites texanus (Figure 11). Detailed foraminiferal micropaleontological analysis was achieved by correlating the identified forms with stratigraphically important Cretaceous arenaceous Benthic Foraminifera of the study area propounded by [22].

Various types of dispersed organic matter and palynomorph groups were identified (Figures 11-13) based on systematics described by several authors [23] [24] [25] [26]. Identified palynomorphs included spores and pollen, fungal remains, freshwater algae, marine palynomorphs (dinoflagellates, acritarchs, micro foraminiferal inner linings), structured phytoclasts (wood, cuticles, parenchyma), unstructured phytoclasts (resins, comminuted and degraded fragments), black debris, and amorphous organic matter following the template of [11].

Lithofacies interpretation forms the primary tool for identifying the depositional conditions under which the sediments were deposited and preserved.

Various lithofacies can be grouped as architectural elements, which are characterized by distinctive facies assemblages, internal geometry, external form and vertical profile [27] [28]. The recognition of these architectural elements, their inherent characteristics and relationships, aided the interpretation of the local and regional processes of deposition in the study area. The lithofacies types identified in the study included:

Cross-bedded sandstone facies (A), Massive sandstone facies (B), Mudstone facies (C), Bioturbated sandstone facies (D), Trough cross-bedded sandstone facies (E), Laminated calcareous shale facies (F), Shale and siltstone facies (G), Shale and mudstone facies (H), Very fine laminated sandstone and siltstone facies (I).

Sediments in lithofacies A and D are cross bedded and heavily bioturbated with Ophiomorpha burrows. The presence of these structures indicates tidal processes with high energy [29] [30] [31]. However, the presence of lateral accretion surface within the studied sandstone sediments suggests fluvial action [28] [29] [30]. These field observations showed that the studied sediments were deposited under tidal and fluvial channels’ interaction as usually seen in littoral environments. The planar cross bedded sandstone facies is interpreted as traction current deposits. Medium-scale planar cross bedding resulted from the preservation of straight crested dunes and sand waves and transverse bars [31] [32]. Whereas strongly bioturbated sandstones with abundant Skolithos and Ophiomorpha traces probably represented the upper shoreface and foreshore environments of deposition (EOD) [33] [34] [35] [36].

The massive sandstone facies (B) is interpreted as a water-laid deposit. Most longitudinal bars are stable bedforms at flood stage, when all the bed loads are in motion. The absence of horizontal lamination or cross lamination typically formed by traction could be due to influence of grain flow depositional process [27]. The mudstone facies (C) comprises light grey and brown mudstone. It is sandy and carbonaceous with commuted plant remains. This facies is in all probability a suspension deposit. The characteristic minute grains and good sorting favour transportation in, and deposition from suspension [9] [37].

Alternating thin units of fine laminated sandstones and siltstones of lithofacies (I) suggests rhythmic sedimentation [38] and the fact that these alternating units have wave ripple laminations, lenticular and flaser bedding, indicates that there were frequent fluctuations in current strength. Such conditions are common in sub tidal and intertidal settings [39].

The Trough cross-bedded sandstone facies (E) is interpreted as a unidirectional traction current deposit [40] [41]. The presence of carbonaceous materials and fissile structure of the laminated shale facies (F) as observed from the field data suggests deposition in shelf to shoreface environment [42] [43].

The composite facies relationship diagrams constructed for the respective formations was used as a basis for interpretation of facies in terms of environment of deposition (EOD). The FRDs showed the dominance of facies (H, D, I) assemblage. It also showed the restriction of this facies assemblage to the basal portion of both stratigraphic sections. The stratigraphic succession in Km 75, Ihube showed that the shale-mudstone facies (H) is usually overlain by the bioturbated sandstone facies (D), laminated sandstone-siltstone facies (I) then Trough cross-bedded sandstone facies (E) except in the up section where the assemblage was succeeded by massive sandstone facies, cross bedded sandstone facies and laminated black shale. In the Ikpankwu quarry section, the basal portion is also characterized by the H, D, I assemblage whereas in the up section, it is replaced by the G and I assemblages comprising of Shale-siltstone facies and fine laminated sandstone siltstone facies. These affinities did not only signify similar depositional processes but also established similar and spatially correlatable lithostratigraphic units (formations) in the study area. In other words, lithofacies assemblage affinities established that the basal and upper lithostratigraphic units in both sections were the Mamu and Nsukka Formations, respectively.

The result of foraminiferal analysis reveals that the study area is rich in benthonic forams, but devoid of planktics. The absence of planktonic foraminifera in the samples, attest and confirm shallow and probably harsh ecological factors [32]. Biostratigraphic data of studied shale samples showed that the Nsukka Formation at Km 75 Enugu-Port Harcourt, Ihube and the upper parts of the section at Ikpankwu were dominated by Haplophragmoides species including (H. Hausa and H. Sahaliense) Trochamina dutsun, Anomalinoides midwayaensis and Ammobaculites anabiensis. That of the Mamu Formation constituting the basal part of the section at Ikpankwu quarry is dominated by Haplophragmoides Species including (H. Saheliense and H. Talokaensis), Ammobaculites texanus. These species assemblages define the age range of Maastrichtian, especially, between Campanian-Maastrichtian and Late Maastrichtian-Paleocene for Mamu Formation and Nsukka Formation sediments, respectively [20] [44]. The formation Fossil, Ammoastuta assemblages, consisting of Ammoastuta, Ammobaculites, Haplophragmoides, Trochammina and others have been described from the Coniacian to Turonian foraminifera from Ashaka northeastern Nigeria [40] , where they were interpreted to be of brackish lagoonal to marsh origin.

Paleoenvironmental interpretations were also carried out based on the abundance and diversity of the micro fauna encountered and the presence of environmentally significant fauna. These sediments were interpreted to be deposited within a Non-marine (Coastal Deltaic) to middle neritic paleo-water depths. These paleobathymetric depth ranges when compared with the bathymetric ranges used in paleoenvironmental interpretations indicated that the sediments were deposited in marginal marine to shallow marine environments [21].

Palynomorphs study of samples in the study area showed that samples from Nsukka Formation at Km 75 Enugu-Port Harcourt road, Ihube and the upper parts of the section at Ikpankwu are characterized by forms such as Leiotriletes adrennis, Retitricolporites annulatus, ongapertites sp., Trifossa pollenites sp., Apectodinium sp., Ephedripites sp., Noothofaqidites sp., Hexaporotricolpites. Some organic walled micro planktons such as Dinogymnoids indet were also found. The shale at the basal parts of the Ikpankwu quarry section, is characterized on the other hand by forms such as Retitrcolporites annulatus, Spinizoncolpites echinatus, Lycopodiumsporites sp, Emelianova, and Foram lining. These assemblages at the basal and upper sections suggest Campanian-Maastrichtian and late Maastrichtian-Paleocene age indicative of Mamu and Nsukka Formation sediments respectively [45] [46] [47].