<?xml version="1.0" encoding="UTF-8"?><!DOCTYPE article  PUBLIC "-//NLM//DTD Journal Publishing DTD v3.0 20080202//EN" "http://dtd.nlm.nih.gov/publishing/3.0/journalpublishing3.dtd"><article xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" dtd-version="3.0" xml:lang="en" article-type="research article"><front><journal-meta><journal-id journal-id-type="publisher-id">MSA</journal-id><journal-title-group><journal-title>Materials Sciences and Applications</journal-title></journal-title-group><issn pub-type="epub">2153-117X</issn><publisher><publisher-name>Scientific Research Publishing</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.4236/msa.2012.311109</article-id><article-id pub-id-type="publisher-id">MSA-24720</article-id><article-categories><subj-group subj-group-type="heading"><subject>Articles</subject></subj-group><subj-group subj-group-type="Discipline-v2"><subject>Chemistry&amp;Materials Science</subject></subj-group></article-categories><title-group><article-title>
 
 
  Ductile Fracture Characterization for Medium Carbon Steel Using Continuum Damage Mechanics
 
</article-title></title-group><contrib-group><contrib contrib-type="author" xlink:type="simple"><name name-style="western"><surname>tergios</surname><given-names>Pericles Tsiloufas</given-names></name><xref ref-type="aff" rid="aff1"><sup>1</sup></xref><xref ref-type="corresp" rid="cor1"><sup>*</sup></xref></contrib><contrib contrib-type="author" xlink:type="simple"><name name-style="western"><surname>Ronald</surname><given-names>Lesley Plaut</given-names></name><xref ref-type="aff" rid="aff1"><sup>1</sup></xref><xref ref-type="corresp" rid="cor1"><sup>*</sup></xref></contrib></contrib-group><aff id="aff1"><addr-line>Department of Metallurgical and Materials Engineering, Escola Politécnica, University of S?o Paulo, S?o Paulo, Brazil</addr-line></aff><author-notes><corresp id="cor1">* E-mail:<email>tsiloufas@usp.br(TPT)</email>;<email>rlplaut@usp.br(RLP)</email>;</corresp></author-notes><pub-date pub-type="epub"><day>27</day><month>11</month><year>2012</year></pub-date><volume>03</volume><issue>11</issue><fpage>745</fpage><lpage>755</lpage><history><date date-type="received"><day>August</day>	<month>2nd,</month>	<year>2012</year></date><date date-type="rev-recd"><day>September</day>	<month>3rd,</month>	<year>2012</year>	</date><date date-type="accepted"><day>October</day>	<month>2nd,</month>	<year>2012</year></date></history><permissions><copyright-statement>&#169; Copyright  2014 by authors and Scientific Research Publishing Inc. </copyright-statement><copyright-year>2014</copyright-year><license><license-p>This work is licensed under the Creative Commons Attribution International License (CC BY). http://creativecommons.org/licenses/by/4.0/</license-p></license></permissions><abstract><p>
 
 
  This paper presents the ductility characterization for a medium carbon steel, for two microstructural conditions, that has been evaluated using the continuum damage mechanics theory, as proposed by Kachanov and developed by Lemaitre. Tensile tests were carried out using loading-unloading cycles in order to capture the gradual deterioration of the elastic modulus, which may be linked to the ductile damage increase with increasing plastic strain. The mechanical parameters for the isotropic damage evolution equation were obtained and then used as inputs for a plasticity-damage coupled nu- merical algorithm, validated through numerical simulations of the experimental tensile tests. A comparison between the SAE 1050 steels studied and two carbon steel alloys (obtained from the literature), provided some basic understanding of the influence of the carbon level on the evolution of the damage parameters. An empiric relationship for this set of parameters, which can provide useful data for preliminary studies envisaging prediction of ductile failure in carbon steels, is also presented.
 
</p></abstract><kwd-group><kwd>Continuum Damage Mechanics; Tensile Testing; Numerical Simulation; Medium Carbon Steels</kwd></kwd-group></article-meta></front><body><sec id="s1"><title>1. Introduction</title><p>Ductile fracture is the failure of a solid material due to nucleation, coalescence and growth of cavities induced by plastic deformation. There are several ways, from empiric relationships [1,2] to porous media stiffness modeling [<xref ref-type="bibr" rid="scirp.24720-ref3">3</xref>], developed to study this phenomenon in order to predict when a workpiece will fail under a given stressstrain state.</p><p>Kachanov, in 1958 [<xref ref-type="bibr" rid="scirp.24720-ref4">4</xref>], first proposed a continuum damage variable to represent the surface density of cavities in a given infinitesimal volume element. By the 70’s, researchers embraced the idea and developed a theory based on the framework of irreversible processes thermodynamics to model the evolution of this damage variable and how it affects mechanical properties, such as elastic modulus and stresses, leading to the eventual failure of a material [<xref ref-type="bibr" rid="scirp.24720-ref5">5</xref>]. This theory, called Continuum Damage Mechanics (CDM), is complementary to Fracture Mechanics, since it is concerned about the nucleation and growth of cavities until they reach a critical size turning into a macroscopic crack, whose propagation in a solid media is studied by the latter.</p><p>For damage evolution caused by large plastic deformation, Lemaitre and Chaboche developed the first and simplest model [6-10], which considers a linear evolution of isotropic damage with plastic strain in a uniaxial stress state condition. This model was later expanded by other authors, adding new capabilities such as dealing with anisotropic damage [<xref ref-type="bibr" rid="scirp.24720-ref11">11</xref>], or with non-linear damage evolution [12-16].</p><p>Recently, medium carbon steel heat-treated to obtain spheroidized cementite in its microstructure is being used as raw material for sheet forming processes, due to its better formability properties [<xref ref-type="bibr" rid="scirp.24720-ref17">17</xref>]. Due to large plastic strains imposed to this kind of manufactured parts, cracks and other defects observed are mostly related to ductile damage evolution.</p><p>With this motivation, in this work the ductile fracture of SAE 1050 steel was studied, for two different microstructural conditions namely: lamellar ferrite-pearlite and spheroidized cementite, under the continuum damage mechanics point of view. Experimental characterization of isotropic damage evolution was carried out and numerical simulations were performed in order to predict failure.</p></sec><sec id="s2"><title>2. Continuum Damage Mechanics Model for Ductile Fracture</title><p>The continuum damage variable introduced by Kachanov is defined as the relationship between the sectional area of voids <img src="1-7700850\ae145249-8ce9-4bd8-9220-16b7cb600348.jpg" /> and the overall sectional area <img src="1-7700850\d77ef7fb-3a86-4459-b3c2-6820e68f28fa.jpg" /> of a given surface in a volume element. Assuming the hypothesis of isotropic deterioration of the material, the damage can be written as:&#160;&#160;&#160;&#160;</p><disp-formula id="scirp.24720-formula12813"><label>(1)</label><graphic position="anchor" xlink:href="1-7700850\809f7e76-8ec8-4f66-8d5f-ebe7ab818c74.jpg"  xlink:type="simple"/></disp-formula><p>where <img src="1-7700850\e3aa0644-6350-4fe2-abe4-df76bfc697fa.jpg" /> is the effective resisting area. It may be observed that this definition is the same one as the microvoid area fraction used is some micromechanical theories, such as McClintock’s [<xref ref-type="bibr" rid="scirp.24720-ref18">18</xref>]. The damage variable can assume any value between 0 and 1, covering from a virgin state to a completely damaged one, although real materials will fail when the damage reaches a critical value<img src="1-7700850\1a14e253-3ba4-4417-b423-8fa99f8dfcba.jpg" />, when the effective area can no longer resist the applied load, leading to the formation of a macroscopic crack.</p><p>In his model, Lemaitre assumes the hypothesis of strain equivalence, which states that the damaged material will have the same constitutive behavior of the virgin material, replacing the stress tensor <img src="1-7700850\c9a55843-c83f-46a3-af67-ecad2daf1f56.jpg" /> by the effective stress tensor<img src="1-7700850\7ecc4f0f-140f-417b-9e55-927a52856de5.jpg" />, defined as:</p><disp-formula id="scirp.24720-formula12814"><label>(2)</label><graphic position="anchor" xlink:href="1-7700850\641a60d3-6436-40d4-8447-4065a7a381fb.jpg"  xlink:type="simple"/></disp-formula><p>One important consequence of this assumption is that one can define an effective elastic modulus of a damaged material, giving an indirect way to measure the damage in a solid, by monitoring the evolution of the Young modulus with increasing strain:</p><disp-formula id="scirp.24720-formula12815"><label>(3)</label><graphic position="anchor" xlink:href="1-7700850\09c63721-65a5-4bed-8fde-a9c4f795b1c3.jpg"  xlink:type="simple"/></disp-formula><p>where <img src="1-7700850\4d5efd57-1f6d-473a-9421-2dc12f4a2555.jpg" /> is the effective elastic modulus and <img src="1-7700850\16e1af90-f3d2-4bb7-828b-63ffd04ae9c2.jpg" /> is the elastic modulus for the undamaged material.</p><p>Using as basis the thermodynamic of irreversible processes [<xref ref-type="bibr" rid="scirp.24720-ref19">19</xref>], CDM treats the damage as an internal thermodynamic state variable, and so its evolution can be derived assuming the existence of a potential of dissipation <img src="1-7700850\bf8433b6-3052-4aa1-a566-7e36ea134dd6.jpg" /> and an associated variable Y, named damage strain energy release rate and defined as [<xref ref-type="bibr" rid="scirp.24720-ref10">10</xref>]:</p><disp-formula id="scirp.24720-formula12816"><label>(4)</label><graphic position="anchor" xlink:href="1-7700850\1e99bb6e-e368-49f6-8a81-02c0ea8fdab3.jpg"  xlink:type="simple"/></disp-formula><p>where <img src="1-7700850\9b656bf1-1bf5-4b69-96cf-b6c811bef6b4.jpg" /> is the von Mises equivalent stress, <img src="1-7700850\b77e4c4e-46c6-4768-a8b1-72dd9a118234.jpg" />is the deviatoric stress tensor, <img src="1-7700850\c0df1274-8ff7-4c22-b2da-38d800b7ce0f.jpg" />is the Poisson’s ratio and <img src="1-7700850\7f7ec19d-221b-4b07-af8c-1a952e757072.jpg" /> is the hydrostatic stress. Further, Lemaitre [<xref ref-type="bibr" rid="scirp.24720-ref10">10</xref>] shows that the damage evolution can be written as:</p><disp-formula id="scirp.24720-formula12817"><label>(5)</label><graphic position="anchor" xlink:href="1-7700850\775bb0cc-5ca1-4b76-9f39-698edba22012.jpg"  xlink:type="simple"/></disp-formula><p>with <img src="1-7700850\5c9db0cb-e47c-4b2e-843a-781dba908c75.jpg" /> defined as the accumulated plastic strain and <img src="1-7700850\658f45d5-deea-486c-bd34-b20ff656b879.jpg" /> being the plastic strain tensor. The choice of a proper potential of dissipation that can represent experimental results is the core of any CDM model. In Lemaitre and Chaboche’s model, the hypothesis of isotropic damage, existence of a strain threshold for damage initiation and linear evolution of the damage with the accumulated plastic strain leads to the following equation for damage evolution:</p><disp-formula id="scirp.24720-formula12818"><label>(6)</label><graphic position="anchor" xlink:href="1-7700850\8ffca97c-7c98-48fc-b023-a76180e022fe.jpg"  xlink:type="simple"/></disp-formula><p>where <img src="1-7700850\65ed38e8-f606-40a1-a405-e9e811b597f5.jpg" /> is the accumulated plastic strain threshold and S is the damage resistance parameter, which are material dependent properties. For the uniaxial stress state, and assuming that the elastic strain can be neglected in comparison to the total strain, the accumulated plastic strain can be considered equal to the principal strain. The damage increases until it reaches a critical value <img src="1-7700850\f09e7766-5e35-4467-9df2-76cbcfbac2e1.jpg" /> which can be calculated with the following equation [<xref ref-type="bibr" rid="scirp.24720-ref10">10</xref>]:</p><disp-formula id="scirp.24720-formula12819"><label>(7)</label><graphic position="anchor" xlink:href="1-7700850\6d9bafca-6f7f-4b91-ba37-e7e8c992eef9.jpg"  xlink:type="simple"/></disp-formula><p>where <img src="1-7700850\d80e96af-94d4-4b40-af47-8b85692e6bed.jpg" /> is the critical damage for the uniaxial stress state and can be measured in a tensile test, <img src="1-7700850\f2531a41-21aa-4d9a-b549-6b532c1b2fe6.jpg" />is the ultimate tensile stress and</p><p><img src="1-7700850\e177975a-c821-40a7-b036-8debde09d31c.jpg" /></p><p>is called triaxiality factor, which accounts for the difference between the actual stress state and the perfectly uniaxial stress state.</p><p>This model was later implemented in the Abaqus/Explicit solver using the VUMAT subroutine [<xref ref-type="bibr" rid="scirp.24720-ref20">20</xref>] following the numerical algorithm proposed by Lee and Pourboghrat [<xref ref-type="bibr" rid="scirp.24720-ref21">21</xref>].</p></sec><sec id="s3"><title>3. Experimental Procedure</title><p>In order to determine mechanical properties and damage parameters, standard tensile tests were carried out for specimens of SAE 1050 steel for the lamellar and for the spheroidized microstructures. Three specimens for the hot rolled ferrite-pearlite material and nine specimens for the spheroidized material were tested.</p><p>The spheroidized material has been cold rolled, with a thickness reduction of 50% and subsequently annealed at 700˚C for 13 hours in a 100% H<sub>2</sub> atmosphere, to obtain the characteristic spheroidized microstructure. The specimens were machined from a 1.0 mm thickness sheet (spheroidized material) and from a 2.0 mm thickness sheet (hot rolled material. The neck section had 75 mm length and 12.5 mm width, as shown in <xref ref-type="fig" rid="fig1">Figure 1</xref>.</p><p>The damage variables were calculated using the variation of the elastic modulus, so several loading-unloading cycles were needed in order to measure this property with strain increase. The tests were performed in an Instron 3369 universal testing machine, with a 50 kN load cell. Each cycle began with a 1 mm crosshead displacement followed by an unloading until the force attained 50 N. The crosshead velocity was fixed at 2 mm/min. The strains were measured through a clip gage extensometer with 50 mm gage length. Sampling frequency was 5 Hz. <xref ref-type="fig" rid="fig2">Figure 2</xref> illustrates the experimental setup.</p><p><xref ref-type="fig" rid="fig3">Figure 3</xref> shows the true stress-strain curves for both types of tested specimens. The loading-unloading cycles shown were used in the evaluation of the elastic modulus, measured always during the unloading path, following recommendations by Lemaitre [<xref ref-type="bibr" rid="scirp.24720-ref10">10</xref>]. The drop in the true stress, as pictured in this figure, can be linked to the fracture initiation. To represent the work hardening behavior of the material, Ludwik equation [<xref ref-type="bibr" rid="scirp.24720-ref22">22</xref>] has been used, as presented by Equation (8). The material constants are given in <xref ref-type="table" rid="table1">Table 1</xref>.</p><disp-formula id="scirp.24720-formula12820"><label>(8)</label><graphic position="anchor" xlink:href="1-7700850\bc3fdbff-f37e-4174-b0bb-39974cde6afb.jpg"  xlink:type="simple"/></disp-formula><p>The evolution of the elastic modulus is shown in <xref ref-type="fig" rid="fig4">Figure 4</xref> for the tested materials (including the pure iron results [<xref ref-type="bibr" rid="scirp.24720-ref23">23</xref>] and other carbon steels [24,25] obtained from the literature). It may be observed that the elastic modulus decreases with increasing carbon level. Also, there is a significant non-linear drop in the elastic modulus for small strains, followed by a linear evolution. Lemaitre’s model considers that the damage does not occur for a strain below the critical value, and will grow with a constant rate after that value. For this reason, following the same procedure of Celentano et al. [<xref ref-type="bibr" rid="scirp.24720-ref24">24</xref>], any elastic modulus degradation below the linear part of the curve will be neglected. This transition coincides with the transition of the elastic regime to the plastic behavior of the material. Therefore, yielding strain will be considered as the damage strain threshold and the elastic modulus, at this point, will be assumed to be the one for the undamaged material.</p><p>The damage evolution, measured trough Equation (3), is shown in <xref ref-type="fig" rid="fig5">Figure 5</xref> for both studied alloys. Critical damage <img src="1-7700850\d8def3c0-b65a-498c-b4cb-c1a21890ee57.jpg" /> is taken as the damage value prior to the non-linear increase in damage, just before fracture. The</p><p>other parameter to be evaluated is the damage resistance S, calculated trough Equation (9), which is obtained by manipulating Equation (6) and assuming that in the tensile test the material is under a perfectly uniaxial stress state.</p><disp-formula id="scirp.24720-formula12821"><label>(9)</label><graphic position="anchor" xlink:href="1-7700850\7b613357-dee3-4e05-a92a-8cd90bc35b9f.jpg"  xlink:type="simple"/></disp-formula><p>To obtain the value of S, several experimental points must be taken from Figures 3 and 5 for different strains.</p><p><xref ref-type="table" rid="table1">Table 1</xref> summarizes the mechanical and damage parameters identified for SAE 1050 steel for both microstructural conditions.</p><p>It must be pointed out that these parameters can be used as inputs for finite element simulations of the tensile test.</p></sec><sec id="s4"><title>4. Numerical Simulations</title><p>Lemaitre’s model was implemented in Abaqus/Explicit finite element solver using a VUMAT subroutine aiming at the coupling of isotropic plasticity with damage, based on the stress integration algorithm called operator-split.</p><p>For each time step, the incremental strain was considered as being fully elastic, and then the corresponding stress tensor was evaluated. The von Mises criterion, coupled with damage, was used to determine if the material is indeed below the yielding condition:</p><disp-formula id="scirp.24720-formula12822"><label>(9)</label><graphic position="anchor" xlink:href="1-7700850\3b4233fd-7398-4268-a5df-0b1c3052f90c.jpg"  xlink:type="simple"/></disp-formula><p>If Equation (10) is not satisfied, then a plastic correcting procedure must be used to calculate the plastic increment and ensure the consistency condition. Details of this plastic corrector can be found in Lee and Pourboghrat [<xref ref-type="bibr" rid="scirp.24720-ref22">22</xref>]. After this calculation, stresses, the damage variable and the plastic strain are updated for the next step. Further details may be obtained in Tsiloufas [<xref ref-type="bibr" rid="scirp.24720-ref26">26</xref>].</p><p>The tensile test was simulated using an imposed longitudinal displacement on the right end of the specimen, with the same 2 mm/min velocity as for the experimental procedure. Boundary conditions of restricted transversal</p><p>and normal displacement were imposed for both ends of the specimen, simulating the jaws of the tensile test equipment. The mesh in the test region is formed by 4500 solid hexahedral elements, with 8 nodes, linear integration and 0.5 mm length.</p><p><xref ref-type="fig" rid="fig6">Figure 6</xref> shows the resulting true stress-strain curves. 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