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Macrae, C.F., Edgington, P.R., McCabe, P., Pidcock, E., Shields, G.P., Taylor, R., Towler, M. and van de Streek, J. (2006) Mercury: Visualization and analysis of crystal structures. Journal of Applied Crystallography, 39, 453-457. http://dx.doi.org/10.1107/S002188980600731X

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• TITLE: Synthesis, crystal structure, and catalytic properties of 2,2’-bipyridyl-dicyano-palladium(II)

  AUTHORS: Xiaoli Tang, Longguan Zhu

  KEYWORDS: Synthesis; Thioanisol; Pd Complex; Oxidation of Sulfide; Hydrogen Peroxide; Disproportionation

  JOURNAL NAME: Open Journal of Inorganic Chemistry, Vol.3 No.4, October 11, 2013

  ABSTRACT: In the solvothermal condition, a Pd(II) complex with a in situ synthesis ligand, [Pd(2,2’-bipy)2(CN)2] (1) was obtained and characterized by elemental analysis, IR, UV, TG, and powder X-ray analysis. The single crystal X-ray analysis showed that the title complex is different from the reported 2,2’-bipyridyl-dicyanopalladium(II) (2) in crystal system and structural parameters. The catalytic investigation for the reactions of the disproportionation of hydrogen peroxide and oxidation of sulfide showed that the complex 1 is an active homogeneous catalyst in the presence of imidazole and 2-sulfobenzoic acid, respectively.