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G. J. Wilson, A. S. Matijasevich, D. R. G. Mitchell, J. C. Schulz and G. D. Will, “Modification of TiO2 for Enhanced Surface Properties:? Finite Ostwald Ripening by a Microwave Hydrothermal Process,” Langmuir, Vol. 22, No. 5, 2006, pp. 2016-2027. doi:10.1021/la052716j

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• TITLE: Photoluminescent Properties of CoMoO4 Nanorods Quickly Synthesized and Annealed in a Domestic Microwave Oven

  AUTHORS: Ana P. de Moura, Larissa H. de Oliveira, Paula F. S. Pereira, Ieda L. V. Rosa, Máximo S. Li, Elson Longo, José A. Varela

  KEYWORDS: Photoluminescence; Nanorods; Molybdates; Microwave-Hydrothermal Method

  JOURNAL NAME: Advances in Chemical Engineering and Science, Vol.2 No.4, November 1, 2012

  ABSTRACT: A simple way to prepare α- and β-CoMoO4 nanorods is reported in this paper. CoMoO4xH2O nanorod precursors were obtained using the microwave-assisted hydrothermal (MAH) method. By annealing the as-prepared CoMoO44xH2O precursor at 600℃ for 10 min in a domestic microwave oven, α- and β-CoMoO4 nanorods were prepared. These powders were analyzed by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), Fourier transform Raman microscopy and ultraviolet visible absorption spectroscopy (UV-vis spectra) as well as photoluminescence (PL) measurements. Based on the results, these materials revealed nanorod morphology. PL spectra obtained at room temperature for α- and β-CoMoO4 particles exhibited maximum components around the blue light emission. The results show that the domestic microwave oven has been successfully employed to obtain α- and β-CoMoO4 nanoparticles.