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A. Dierstein, H. Natter, F. Meyer, H. O. Stephan, C. Kropf and R. Hempelmann, “Electrochemical Deposition under Oxidizing Conditions (EDOC): A New Synthesis for Nanocrystalline Metal Oxides,” Scripta Materialia, Vol. 44, No. 8-9, 2001, pp. 2209-2212.doi:10.1016/S1359-6462(01)00906-X

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• TITLE: Facile Synthesis and Characterization of Nanoporous NiO with Folic Acid as Photodegredation Catalyst for Congo Red

  AUTHORS: Faezeh Farzaneh, Sara Haghshenas

  KEYWORDS: Nanoporous NiO; Photodegredation; Congo Red; Folic Acid

  JOURNAL NAME: Materials Sciences and Applications, Vol.3 No.10, October 22, 2012

  ABSTRACT: In this study nanoporous NiO was prepared using Ni(CH3COO)2,4H2O, folic acid and water as starting material, template and solvent respectively, by sol gel method followed by calcination at 400℃. The solid product was characterized by X-ray diffraction (XRD), nitrogen adsorption-desorption, scanning electron microscopy (SEM), transmission electron microscopy (TEM) Fourier transform infrared (FT-IR) and photoluminescence (PL) techniques. The particle size of the nanoparticles estimated by XRD was in good agreement with the particle size obtained by TEM analysis (4-5nm). It was also found that the prepared nanoporous NiO show very good activity for photodegredation of dye organic pollutants such as Congo red (91%) during 1.5 hours.