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F. H. Allen, O. Kennard, D. G. Watson, L. Brammer and A. G. Orpen, “Tables of Bond Lengths Determined by X-Ray and Neutron Diffraction. Part 1. Bond Lengths in Organic Compounds,” Journal of the Chemical Society, Perkin Transactions II, Vol. 12, 1987, pp. S1-S19. doi:10.1039/p298700000s1

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• TITLE: Unusual Catalytic Process Involving OH and NH Exchange

  AUTHORS: Ramadan M. Ramadan, Ahmad K. Abu Al-Nasr

  KEYWORDS: Bicompartment Ligand; Schiff Bases; Diaminobenzene; X-Ray Analysis

  JOURNAL NAME: International Journal of Organic Chemistry, Vol.2 No.1, March 15, 2012

  ABSTRACT: Interaction of some transition metals species with a Schiff base, 1, derived from 4,6-diacetylresorcinol and 2-amino- 5-methylphenol (1:2 mole ratio) yielded the two compounds 4-ethanimidoyl-6-[(1E)-N-(2-hydroxy-4-methylphenyl) ethanimidoyl]benzene-1,3-diol, 2, and 4,6-diacetyl-1,3-diaminobenzene, 4 via unusual catalytic process involving OH and NH exchange. All the compounds are characterized by elemental analysis, IR, mass and 1H NMR. The structure of the two compounds 2 and 4 are also determined by X-ray analysis. The crystal structure analysis revealed that the two compounds crystallized in the monoclinic space group P21/c with a Z value of 4.