Article citationsMore>>

S. C. Cunha, J. O. Fernandes, A. Alves and M. Oliveira, “Fast Low-pressure Gas Chromatogra-phy-Mass Spectro- metry Method for the Determination of Multiple Pesti- cides in Grapes, Musts and Wines,” Journal of Chroma- tography A, Vol. 1216, No. 1, 2009, pp. 119-126. doi:10.1016/j.chroma.2008.11.015

has been cited by the following article:

• TITLE: Fast Determination of 22 Pesticides in Rice Wine by Dispersive Solid-Phase Extraction in Combination with GC-MS

  AUTHORS: Nannan Chen, Hongbo Gao, Nengsheng Ye, Qiding Zhong, Zhenghe Xiong, Xuexin Gu

  KEYWORDS: d-SPE; Rice Wine; Pesticide; GC-MS; Matrix Effect

  JOURNAL NAME: American Journal of Analytical Chemistry, Vol.3 No.1, January 5, 2012

  ABSTRACT: A rapid method was developed for the determination of 22 pesticides in rice wine. The procedure involved an extraction with acetonitrile and a cleanup step using dispersive solid-phase extraction (d-SPE), and primary-secondary amine (PSA) and octadecylsilane (ODS) were used as sorbents. D-SPE had some advantages over some traditional prepara- tions, especially in time and cost. Both the extraction and cleanup only cost about 15 min per a sample. Then the GC-MS was used for quantitative and qualitative analysis. Matrix-matched standards solution and analyte protectant were compared to decrease the matrix effect, and the former showed a better efficacy. Acceptable linearity was achieved in the range of 0.05 - 0.30 mg/L. After matrix-matched standards calibration, recoveries were between 60 and 140%. For the most of pesticides, precision and repeatability were less than 10% and 16%, respectively. The result indicated that the developed method was suitable for the determination of the multi-pesticides in rice wine.