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Miriyala, B. Bhattacharyya, S. and Williamson, J. S. (2004) Chemoselective reductive alkylation of ammonia with carbonyl compounds: synthsis of primary and sym-metrical secondary amines. Tetrahedron, 60, 1463-1471,.

has been cited by the following article:

• TITLE: A validated, related substance, GC method for 1,4-cyclohexanedione mono-ethylene Ketal

  AUTHORS: B. Karthikeyan, V. Srinivasan

  KEYWORDS: Column Gas Chromatography; 1, 4-Cyclohexanedione Mono-Ethylene Ketal; 1, 4-Cyclohexanedione Bis (Ethylene Ketal); Validation

  JOURNAL NAME: Journal of Biophysical Chemistry, Vol.1 No.1, June 1, 2010

  ABSTRACT: ABSTRACT A simple, economic, and time-efficient related substance, GC method has been developed for the analysis of 1,4-Cyclohexanedione mono- ethylene ketal(will be specified as ketal) in the presence of a potential impurity 1,4-cyclohexa- nedione bis (ethylene ketal) [will be specified as diketal]. Successful chromatographic separa- tion of the ketal from the impurity was achieved on a DBWAX ETR, 30 m x 0.32 mm x 1.0μ FT column with nitrogen as carrier gas and FID detector. The method was validated for linearity, accuracy, precision, and specificity and can be used for quality control during manufacture of ketal. A validated GC method is reported for the ketal for the first time.