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D. C. Elias, R. R. Nair, T. M. G. Mohiuddin, S. V. Mo- rozov, P. Blake, M. P. Halsall, A. C. Ferrari, D. W. Boukhvalov, M. I. Katsnelson, A. K. Geim and K. S. Novoselov, “Control of Graphene’s Properties by Reversible Hydrogenation,” Science, Vol. 323, No. 5914, 2009, pp. 610-613. http://dx.doi.org/10.1126/science.1167130
has been cited by the following article:
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TITLE:
Optimization of Micromechanical Cleavage Technique of Natural Graphite by Chemical Treatment
AUTHORS:
Luis Torres, Luis Gomez Armas, Antonio Carlos Seabra
KEYWORDS:
Graphene; Micromechanical Cleavage; Raman Spectroscopy; Chemical Treatment
JOURNAL NAME:
Graphene,
Vol.3 No.1,
January
16,
2014
ABSTRACT: In this work,we report a method to improve the efficiency of the micromechanical cleavage technique to obtain few-layers graphene samples, from natural graphite flakes, which were previously submitted to two chemical treatment times with H2SO4(17 and 25 hours). After the chemical treatment times, Raman spectroscopy reveals a hydrogenation of the few-layer graphene samples, which were obtained from the treated graphite flakes. To analyze the hydrogenation of the samples, the G and 2D bands of the Raman spectra of the treated and un-treated samples were analyzed and compared, as well as the I(2D)/I(G) ratio, revealing a p-doping on the treated samples when compared with the untreated samples. Our studies could be of great importance to obtain larger and greater amount of few-layer graphene samples.